- A facile single crystal to single crystal transition with significant structural contraction on desolvation.
A facile single crystal to single crystal transition with significant structural contraction on desolvation.
Chemical communications (Cambridge, England) (2014-10-11)
Jane V Knichal, William J Gee, Andrew D Burrows, Paul R Raithby, Simon J Teat, Chick C Wilson
PMID25303036
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5-Ethynyl-1,3-benzenedicarboxylic acid (H2ebdc) reacted with lead(II) acetate trihydrate yields a 1D ladder network, [Pb(ebdc)(MeOH)]2ยทH2O (1). Removing crystals of 1 from the mother liquor results in a facile single crystal to single crystal transition, yielding 2D [Pb(ebdc)] net (2) with a change in space group from I2/a to P1ฬ.
MATERIALS
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Lead(II) acetate trihydrate, puriss. p.a., ACS reagent, reag. ISO, reag. Ph. Eur., 99.5-102.0%
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