GC Analysis of ฮฑ-Hexachlorocyclohexane (ฮฑ-HCH) Enantiomers on Astecยฎ CHIRALDEXโข G-DM

CONDITIONS
column
Astec CHIRALDEX B-DM, 30 m x 0.25 mm I.D., 0.12 μm (77023AST)
oven
170 ยฐC
inj. temp.
250 ยฐC
detector
FID, 250 ยฐC
carrier gas
helium, 30 psi
injection
0.2 μL, 80:1 split
sample
2 mg/mL in ethanol
peaks 1 & 2: ฮฑ-HCH (ฮฑ-hexachlorocyclohexane) enantiomers
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CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC