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Merck

GC Analysis of ฮฑ-Hexachlorocyclohexane (ฮฑ-HCH) Enantiomers on Astecยฎ CHIRALDEXโ„ข G-DM

GC Analysis of α-Hexachlorocyclohexane (α-HCH) Enantiomers on Astec® CHIRALDEX™ G-DM suitable for GC

Materials

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Astecยฎ CHIRALDEXโ„ข B-DM Capillary GC Column

L ร— I.D. 30 m ร— 0.25 mm, df 0.12 ฮผm

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HCH

PESTANALยฎ, analytical standard, mixture of isomers (ฮฑ:ฮฒ:ฮณ:ฮด=1:1:1:1)

ฮฑ-HCH

PESTANALยฎ, analytical standard

CONDITIONS

column

Astec CHIRALDEX B-DM, 30 m x 0.25 mm I.D., 0.12 μm (77023AST)

oven

170 ยฐC

inj. temp.

250 ยฐC

detector

FID, 250 ยฐC

carrier gas

helium, 30 psi

injection

0.2 μL, 80:1 split

sample

2 mg/mL in ethanol
peaks 1 & 2: ฮฑ-HCH (ฮฑ-hexachlorocyclohexane) enantiomers

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Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC