technique(s)
HPLC: suitable
solid phase microextraction (SPME): suitable
test parameters
sample/matrix: 3 mL water containing 8ng/mL of each analyte in 10% NaCl
SPME fiber: PDMS/DVB, 60 μm (57317)
extraction: immersion, 40 min, rapid stirring
desorption process: static, 5 min in acetonitrile:water (65:35); dynamic, valve open during run
column: SUPELCOSIL LC-8, 15 cm × 4.6 mm I.D., 5 μm particles (58220-U)
mobile phase: [A] acetonitrile; [B] water
gradient: 18:82 to 65:35 in 9 min, hold 3 min
flow rate: 2.0 mL/min
column temp.: 35 °C
detector: UV, 240 nm
suitability
application for HPLC
application for SPME
application(s)
environmental
Legal Information
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