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core: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
reaction type: Cross Couplings
애플리케이션
Screening kit for Copper C-N Cross-Coupling Reactions. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for KitAlysis™ High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit
Downloadable experimental excel sheet
Each kit contains 2 customizable screening sets that include the following components:
Monitor reaction progress via TLC-MS by following this protocol
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
Step-by-Step Guide for KitAlysis™ High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit
Downloadable experimental excel sheet
Each kit contains 2 customizable screening sets that include the following components:
- 24 (6 x 4) pre-weighed ligands in glass vials loaded with stir bars, topped with cap mat
- Potassium phosphate: 4 pre-weighed vials with product labels and lids
- CuI (soluble source) in preweighed vial
- 4 degassed anhydrous solvents (dioxane, DMAc, toluene, and DMSO) in ampules
- 1 internal standard
- 2 KitAlysis 24-Well reaction block replacement films
- 8 stir bars for stock solutions
- Ampule cracker
Monitor reaction progress via TLC-MS by following this protocol
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
특징 및 장점
- Designed and tested by synthetic chemists.
- Easily run 24-microscale reaction in parallel.
- Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
- Customizable and downloadable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.
법적 정보
KitAlysis is a trademark of Sigma-Aldrich Co. LLC
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Danger
Hazard Classifications
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 1B - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3
표적 기관
Central nervous system, Respiratory system
보충제 위험성
Storage Class Code
3 - Flammable liquids
Flash Point (°F)
39.2 °F
Flash Point (°C)
4 °C
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