GC Analysis of FAMEs in Mozzarella (Buffalo Milk Source) on SLBยฎ-IL111

Materials
๊ด๋ จ ์ ํ
์ ํ ๋ฒํธ
์ค๋ช
๊ฐ๊ฒฉ
Boron trifluoride-methanol solution
~10% (~1.3 M), derivatization grade (GC derivatization), LiChropurโข๋ถ์ ์ปฌ๋ผ
์ ํ ๋ฒํธ
์ค๋ช
๊ฐ๊ฒฉ
ํ์ค ๋ฌผ์ง
์ ํ ๋ฒํธ
์ค๋ช
๊ฐ๊ฒฉ
F.A.M.E. Column Evaluation Mix
certified reference material, 1000 μg/mL each component in dichloromethaneCONDITIONS
column
SLB-IL111, 100 m x 0.25 mm I.D., 0.20 μm (29647-U)
oven
70 ยบC (4 min), 12 ยบC/min to 160 ยฐC (25 min), 4 ยบC/min to 220 ยบC
inj. temp.
230 ยฐC
detector
FID, 240 ยบC
carrier gas
hydrogen, 40 cm/sec
injection
0.2 μL 10:1 split
sample
FAMEs from 100 mg buffalo milk source mozzarella transesterified in sodium methoxide/methanol + boron trifluoride
์ค๋ช
๋ฒ์ ์ ๋ณด
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany