8.53029
Boc-Glu(OcHx)-OH
Novabiochem®
Synonym(s):
Boc-Glu(OcHx)-OH, N-α-t.-Boc-L-glutamic acid γ-cyclohexyl ester
About This Item
Recommended Products
Quality Level
product line
Novabiochem®
assay
≥98% (TLC)
form
powder
reaction suitability
reaction type: Boc solid-phase peptide synthesis
manufacturer/tradename
Novabiochem®
mp
54-57 °C
application(s)
peptide synthesis
functional group
carboxylic acid
storage temp.
2-30°C
1 of 4
This Item | 8.53052 | 8.53089 | 8.53066 |
|---|---|---|---|
| form powder | form powder | form powder | form powder |
| assay ≥98% (TLC) | assay ≥98% (TLC) | assay ≥98% (TLC), ≥98.0% (HPLC) | assay ≥98% (TLC) |
| functional group carboxylic acid | functional group carboxylic acid | functional group carboxylic acid | functional group carboxylic acid |
| product line Novabiochem® | product line Novabiochem® | product line Novabiochem® | product line Novabiochem® |
| storage temp. 2-30°C | storage temp. 2-30°C | storage temp. 2-8°C | storage temp. 2-30°C |
| mp 54-57 °C | mp 102-105 °C | mp - | mp 110-113 °C (decomposition) |
General description
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] J. P. Tam, et al. (1979) Tetrahedron Lett., 42, 4033.
Linkage
Analysis Note
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in methanol): -9.0 - -7.0 °
Purity (TLC(0811)): ≥ 98 %
Purity (DC (0157)): ≥ 98 %
Solubility (1 mmole in 2 ml DMF): clearly soluble
To see the solvent systems used for TLC of Novabiochem® products please click here.
Legal Information
Storage Class
11 - Combustible Solids
wgk_germany
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
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Protocols
The most popular reagent for cleavage of peptides from Boc-based resins is anhydrous HF. Of all the cleavage procedures HF appears to be the most versatile and least harmful to a wide variety of peptides synthesized on Boc-based resins.
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