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01829

Supelco

Extractables and Leachables Screening Standard for GC

certified reference material, TraceCERT®, 14 components in tert-Butyl methyl ether, Manufactured by: Sigma-Aldrich Production GmbH, Switzerland

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About This Item

UNSPSC Code:
41116107
NACRES:
NA.24
Pricing and availability is not currently available.

grade

certified reference material
TraceCERT®

Quality Level

300

shelf life

limited shelf life, expiry date on the label

manufacturer/tradename

Manufactured by: Sigma-Aldrich Production GmbH, Switzerland

concentration

50 mg/L each component (nominal concentration)

application(s)

pharmaceutical

format

multi-component solution

storage temp.

−20°C

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2-Mercaptoimidazole 98%

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2-Mercaptoimidazole

assay

≥98%

assay

98%

assay

97%

assay

98%

solubility

95% ethanol: soluble 50 mg/mL, clear to very slightly hazy, colorless to yellow, diethyl ether: soluble, propylene glycol: soluble, water: insoluble, benzene: soluble, toluene: soluble, isopropanol: soluble

solubility

methanol: soluble 1 g/10 mL, clear, colorless to very faintly yellow

solubility

toluene: soluble 2.5%, clear, yellow

solubility

methanol: soluble 50 mg/mL, clear to slightly hazy, colorless to yellow

mp

158-160 °C (lit.)

mp

177-179 °C (lit.)

mp

74-77 °C (lit.)

mp

228-231 °C (lit.)

Quality Level

100

Quality Level

200

Quality Level

100

Quality Level

100

General description

This certified reference material (CRM) is produced and certified in accordance with ISO/IEC 17025 and ISO 17034. This CRM is traceable to the SI through a primary reference material from an NMI, e.g. NIST, NRC or NMIJ.
Certified content incl. uncertainty and expiry date are given on the certificate.
Download your certificate at: http://www.sigma-aldrich.com.

Check out our complete range of extractables and leachables certified reference mixes

Application

Extractables Study with GC/MS - Extractables Studies of Single-Use Equipment article from >AnalytixReporter issue 8

Preparation Note

For the preparation of this CRM only materials of highest purity were used.

Legal Information

TraceCERT is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate
    ε-Caprolactam
    2-Mercaptobenzothiazole
    Bisphenol A
    3,5-Di-tert-butyl-4-hydroxytoluene
    1,3-Di-tert-butylbenzene
    Oleamide
    Bis(2-ethylhexyl) phthalate
    Stearic acid
    cis-13-Docosenoamide
    Tris(2,4-di-tert-butylphenyl)phosphate
    2,4-Di-tert-butylphenol
    2,6-Di-tert-butylphenol
    Palmitic acid
    See All (14)

pictograms

FlameExclamation mark
GHS02,GHS07

signalword

Danger

hcodes

H225,H315

Hazard Classifications

Flam. Liq. 2 - Skin Irrit. 2

Storage Class

3 - Flammable liquids

wgk_germany

WGK 1

flash_point_f

-18.4 °F - closed cup

flash_point_c

-28 °C - closed cup

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    Acceptability of thioamides. II. Prothionamide.
    D K Gupta
    Journal of postgraduate medicine, 23(4), 181-185 (1977-10-01)
    A Yilmaz et al.
    Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy, 152, 262-271 (2015-07-29)
    Prothionamide (PTH) is the secondary drug used against Mycobacterium tuberculosis bacteria and leprosy. The aim of this work was to investigate the potential energy surface map, anharmonic and harmonic vibrational spectra, NBO analysis and ELF (Electron Localization Function) of the
    Han-Lin Hsu et al.
    Journal of the Formosan Medical Association = Taiwan yi zhi, 109(12), 923-927 (2011-01-05)
    Timely and intensive monitoring for, and management of, adverse effects caused by anti-tuberculosis drugs are essential components of control programs for multidrug-resistant tuberculosis (MDR-TB). This retrospective case series was conducted in northern Taiwan from January 2007 to December 2008 at
    A case of DRESS syndrome induced by the antituberculosis drugs, prothionamide, and para-aminosalycilic acid.
    Joo-Hee Kim et al.
    Annals of allergy, asthma & immunology : official publication of the American College of Allergy, Asthma, & Immunology, 110(2), 118-119 (2013-01-29)

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